ISO 00813-2-2024.docx

5>×SOInternationa1.StandardISO813-2Firstedition2024-02©ISO2024Rubber,vu1.canizedorthermop1.asticDeterminationofadhesiontoarigidsubstrate一包两.ionofasoftthermop1.astice1.astomer1.ayerCaoutchoucvu1.caniseouthermop1.astiqueDeterminationde!'adherenceaunsuhstratrigide一Partie2:Adherenced,unecouched,e1.astomerethermoPIaStiqUesoup1.eReferencenumberISO813-22024(en)COPYRIGHTPROTECTEDDOCUMENT©ISO2024WintG<hcdBdHUWwdotherwiseCrW4WMrtiwcmbxtt11)ni(WkJhrtRinkHimftWr1.9Htumcnpyip<?IHdiCnticnma),theinternetoranintranet,withoutpriorwrittenpermission.Permissiononber<?qucste<ifromeitherISOattheaddressbe1.oworISOsmemberbodyinthecountryoftherequester.b,Vyfrfiandonnet8CH-1214Vcmicr,GenevaPhoae:*41227490111聊独te:薪括嬴OQrgPub1.ishedinSwitzer1.andContentsPageForeworditroductionv2 SCope13 Normativereferences14 Termsanddefinitions5 Princip1.e2Apparatus25.1 Tensi1.etestingmachine25.2 TTesttro1.1.ey2Testpieces7.1 Formanddimensions7.2 Testpiecefabricationusingtheinjectionmou1.dingmethodConditioning51*estCOnd1.tIonS6Procedure6Expressionofresu1.ts611.1 Pedstrength611«2FractvirePatTem7Testreport8Annex A informative)Examp1.eof1.istingthetestresu1.ts10Annex B (normative)Ca1.ibrationschedu1.e12Annex C (informative)G1.ossarjr14Bib1.iographyISForewordISO(theInternationa1.OrganizationforStandardization)isaWOHdwidefederationofnationa1.standardshUMiest触UimatntenWd泌EMhmvnribefPrbP呷蛔UrteitndtiOna1.StautipndiirRdriobI1.ytecbafrftiatiMDtthtoeghhasbeenestab1.ishedhastherighttoberepresentedonthatcommittee.Internationa1.organizations,governmenta1.andnon-governmenta1.,in1.iaisonwithISO,a1.sotakepartinthework.ISOco1.1.aboratesc1.ose1.ywiththeInternationa1.E1.ectrotechnica1.Commission(IEC)ona1.1.mattersofe1.ectrotechnica1.standardization.Theproceduresusedtodeve1.opthisdocumentandthoseintendedforitsfurthermaintenancearedescribedintheISO/IECDirectives,Part1.Inparti1.ar,thedifferentapprova1.criterianeededforthedifferenttypesISOdrawsattentiontothepossibi1.itythattheimp1.ementationofthisdocumentmayinvo1.vetheuseof（八）儡隔跳淞PeCgke*"斑除ition褪脓膈和席嘛曲膑%懦I挪的酎阳丽小强曲端皂PateMpatents)whichmayberequiredtoimp1.ementthisdocument.However,imp!ementersarecautionedthatthismaynotrepresentthe1.atestinformation,whichmaybeobtainedfromthepatentdatabaseavai1.ab1.eatWWWmeMirgpm1.3NsISOsha1.1.notbehe1.dresponsib1.eforidentifyinganyora1.1.suchpatentrights.Anytradenameusedinthisdocumentisinformationgivenfortheconvenienceofusersanddoesnotconstituteanendorsement.F3mHBxpaMI而Rm收as*M减tuyrURgb11and僦疝U由巾&而ngSgt皿皿JmUm出处如峥但SjOnSOrganization(VVrTO)princip1.esintheTechnica1.BarrierstoTrade(TBT),seewww.iso.org/iso/forcword.htm1.站的byTechnica1.Comnuttce!SOTC45,Rubberandrubberproducts,SubcommitteeA1.istofa1.1.partsintheISO813seriescanbefoundontheISOwebsite.Wpetefebinek)6fc>dockf1.ho11Wtv¼4i11rt<Mnenbertorn1.1.snationa1.standardsbody.AIntroductionNowadaysitiscommontousecombinationsofmateria1.saimedatachievingspecia1.propertiesforpartsfunc11MUct.vi3mstidBipsoantistacti1.e(TPEs)reasons>Mtiinjed碗etpeutdtKKeft)StheSea州Mng1.metfmrdthemajorityofcases.3.4Duetotheirthermop1.asticnature,TPEmateria1.saregainingimportancesteadi1.yinthisareare1.ativetovu1.canizedrubber.刖胸怖5r琳断1.usior三三WM题1如三sstre"价betw用ffWcriat锦刷WJ板,itisthepurposeofthisdomentistospecifyapee1.testprocedurespecifica1.1.yformeasuringtheadhesionOfaTPEtoarigidsubstrate.Rubber,vu1.canizedorthermop1.asticDeterminationofadhesiontoarigidsubstrate一Ma至ionofasoftthermop1.astice1.astomer1.ayerWARNING1Personsusingthisdocumentshou1.dbefami1.iarwithnorma1.1.aboratorypractice.Thisdocumentdoesnotpurporttoaddressa1.1.ofthesafetyprob1.ems,ifany,associatedwithitsuse.Itistheresponsibi1.ityoftheusertoestab1.ishappropriatesafetyandhea1.thpracticesandtodeterminetheapp1.icabi1.ityofanyotherrestrictions.WARNING2Certainproceduresspecifiedinthisdocumentcaninvo1.vetheuseorgenerationofsubstances,orthegenerationofwaste,thatcou1.dconstitutea1.oca1.environmenta1.hazard.Referenceshou1.dbemadetoappropriatedocumentationonsafehand1.inganddisposa1.afteruse.1 ScopeThisdocumentspecifiesatestmethodforassessingthepee1.strengthofathermop1.astice1.astomer(TPE)toarigidsubstrate.Itismain1.yapp1.icab1.etosoftcomponentsintheShoreAhardnessrange.Thisdocumentspecificsatestpiecebutnottheinjectionmou1.dingtoo1.foritsmanufacture.Hence,itispossib1.ethatdifferentresu1.tsareobtainedfortestpiecesproducedusingdifferentinjectionmou1.dingtoo1.s.2 NormativereferencesThefo1.1.owingdocumentsarereferredtointhetextinsuchawaythatsomeora1.1.oftheircontentconstitutesrfeq4item>tifxhhettfrenotd*dodmHhtref<rdcBUpnjthe!urtmsJtaMies.Forundatedreferences,50,十曲政ft够鼬s"cstestequipmentTensi1.e,f1.exura1.andcompressiontypes(constantrateof弼"啊嗓济曲/andp1.asticsAna1.ysisofmu1.ti-peaktracesobtainedindeterminationsOftearstrengthandISO18899:2013,RubberGuidetotheca1.ibrationoftestequipmentB>OTcTJP,91JHrdc1.MH11Sproceduresforpreparingandconditioningtestpiecesforphysica1.testmethodsNotermsanddefinitionsare1.istedinthisdocumentISOandIECmaintaintermino1.ogydatabasesforuseinstandardizationatthefo1.1.owingaddresses：IECE1.cctropcdia:avai1.ab1.ea1.https:/www.e1.ectropedia.org/4Princip1.eseparationbeing90°andthewidthandthicknessoftheTPEbeingfixedwithinspecified1.imits.5Apparatus5.1 Tensi1.etestingmachine5.2 Testtro1.1.eyarrangementFigurepuIIeyzThemotioninmountinghorizonta1.directiondoesthenotexceedrequire<1.tosetthetestDimensionsinmi1.1.imetresdampedtestspecimenguidepu1.1.ey,freerotationSha1.1.bePOSSibIe,FigurediameterTesttro1.1.eymmisrecommendedTheforcerequiredtocauseseparationofastripofaTPEcoveringarigidsubstrateismeasured,theang1.eofSpecia1.TPEmateria1.descriptionsare1.istedinAnnexCforbetterunderstanding.Atensi1.etestingmachineinaccordancewithc1.ass1ofISO5893sha1.1.beusedtoperformthepee1.test.Anexamp1.eofasu¾ubtesttro1.1.eyusedforc1.ampingthetestpieceisshowninFigure1andthec1.ampinginc1.udingtheinguide2.intro1.1.eythesha1.1.besuchthatforce4N.A1.1.dimensionsarejustaguide.Thechosendimensionofthetestspecimensha1.1.fitsecure1.yintothetro1.1.ey.mountingdampingp1.atesa1of8mm91 tensi1.eaxis2 freeendofthesoftcomponent3 guidepu1.1.eydirectionoftheforce山estFH.Ei电&停angement6 Ca1.ibrationThetestapparatussha1.1.beca1.ibratedinaccordancewiththeschedu1.egiveninAnnexB.7 Testpieces7.1 FormanddimensionsThetestpieceshowninFigure3sha1.1.beused.Thestandardwa1.1.thicknessforthesoftcomponentsha1.1.bwfiidscd(iaixtO2)ithe.caseofaTPEwitha1.owhardncssrthesoftcomponentwa1.1.thicknesscanberigidsubstrate2Figure3Testpiece7.2 Testpiecefabricationusingtheinjectionmou1.dingmethodaccordancetechnique.materia1.manufacturersProcessingofinstructions.Therecommendedpre-mou1.dedishardinterruption.Compensatingovermou1.dingSha1.1.ofbepresentcomponentComponentnecessaryJace(strap-side).Possib1.y,exc1.udemeans6050softcomponent23±0,2Thetestpiecessha1.1.preferab1.ybefabricatedusingatwo-componentinjectionmou1.dingmethodincore-backwith4jThetoossurfaceinthethesubsequentbondforthetechniquethecomponentsha1.1.haveasurfaceroughnessofRArangingfrom2,20mto3,20maccordingtoISO21920-1,createdbyerodingthesurface.Thesequenceofeventsinthemou1.dingprocesssha1.1.proceedwithoutA1.1.thesurfacesofthetestpieceshou1.dbefreefromvisib1.edefectssuchasowmarks,sinkmarksandairinc1.usions.Overmou1.dingattheinterfaceregionOfthemateria1.susedshou1.dbeavoidedasfarasofpossib1.e.Noforshrinkingthehardatthehardwi1.1.betsendThetoo1.designsha1.1.atheformationofawe1.d1.ineonthehardcomponent.Notetheexamp1.esofdefectsshowninFigure4.7.3 TestpiecewithinsertedrigidsubstrateTestpieceswitha1.1.typesofrigidsubstratescanbeproducedusingtheinsertiontechnique.7.4 NumberoftestpiecesAt1.eastfivetestpiecessha1.1.betested.Testpiecesa1.readystressedordamagedattheinterfaceregionsha1.1.Gondiitioningf1.1.1.S(Sfhonedforat1.east16hinastandard%ind)sinkmarksc)airinc1.usionse)overmou1.dingattheinterfaceRioe4EXamP用SoVerfIdeW1.itSgatthehardcomponentsendface9 TestconditionsCarryouttestinginastandardatmosphereof(23±2)oC(50±10)%inaccordancewithISO23529.10 ProcedureInsertthetestpiececomp1.ete1.yintothetesttro1.1.eyandfixitinsuchawaythatitcannots1.ideoutofthetro1.1.eyduringtesting.Attachthetro1.1.eytothe1.owermountingofthetestmachine.C1.ampthefreeendofthesoftcomponentintheuppergripsofthetensi1.emachinesuchthatitisatanang1.eof900tothespumu'sinterface,andthe伽明*d*ionC曲外卿Mtotheg遮曜福加e!良USiIeS6银he辨&1.冏斑椀EnSU1.h1.应emountingofthetestpiececanbeachieved,forexamp1.e,byusinganadjustab1.eguiderai1.Thetesttro1.1.eysha1.1.beab1.etomovefree1.ya1.ongitshorizonta1.axisinthec1.ampingsystem.口及腮代砧呼自3Vesrth密MyH出theord骷Par轴翻B怕隔Hh枪g.W"决ndedW住asm包theth(M砂Cepee1.ed.11 Expressionofresu1.ts11.1 Pee1.strength(1)whereFbistheadhesionstrengthinNca1.cu1.atedinaccordancewithISO6133；isthesoftcomponentswidthattheinterfaceinmm.11.2 FracturepatternVisua1.1.yassessthetestpiecefracturepatternusingthec1.assificationSystcnyuwUwthissubc1.ausc.Thedecisivefeatureisthedominantfracturepatternwithoutedgeeffects(seeFigure5).Characterizethenatureofthetestpiecefai1.ureusingoneortwocharactersdescribingthefracturepattern.ThefirstcharacterdescribestheresidueofTPEonthehardCompGnrAt(seeFigure5).ThesecondcharacterdescribeswhereTPEstripfai1.sduringthemeasurement(seeFigure6).AO%TPEresidueontherigidsubstratewithcomp1.etepee1.ing;B(1-50)%TPEresidueontherigidsubstrate;C(51-99)%TPEresidueontherigidsubstrate;DFai1.ureofthesoftcomponentpee1.ed1.engthof1.essthan15mmIsa1.1.owed;A/Dmixedfracturepattern"A"and"D",withfirstA"andthentheTPEstripfai1.ing;B/Dmixedfracturepattern"B"and"D：withfirst*BuandthentheTPEstripfai1.ing;CI)mixedfracturepattern"C"and,)u,withfirst"C"andthentheTPEstripfai1.ing;Esamp1.edestructionwithhardco11poncntrigidsubstrateresidueontheTPE(nofigure).KeyAnoTPEresidueontherigidsubstrateB(1-50)%TPEresidueontherigidsubstrate,noTPEbreakC(51-99)%TPEresidueontherigidsubstrate,noTPEbreakDtomoffmm)samp1.edestruction-softComponcntFigure5(15FracturepatternsDBfDQDKeyB/D(1-50)%TPEresidueontherigidsubstrate；TPEstriptornoffC/D(51-99)%TPEresidueontherigidsubstrate;TPEstriptornoffFigure6FracturepatternscontinuedForfracturepatternsA/D,B/DandC/Dindicatethepee1.ing1.engthbetweenthebeginningandtheTPEstrip4>2tJqst<report6).Thetestreportsha1.1.inc1.udethefo1.1.owinginformation:a) samp1.edetai1.s：afu1.1.1) used;descriptionofthesamp1.eanditsorigininc1.udingtheTPEmateria1.andtherigidsubstrate2) themethodofpreparationofthetestpiecefromthesamp1.einc1.udingthefabricationprocess,injectionmou1.ding/insertmou1.dingandinjectiondirectionofthesoftcomponent;3) thesoftcomponentwa1.1.thickness；4) anydefectspresentonthetestpiece；b) testmethod:1) afu1.1.referencetothetestmethodused,i.e.thisdocument(ISO813-2:2024);c) testdetai1.s:1) the1.aboratorytemperatureandhumidity;2) thetimeandtemperatureandhumidityofconditioningpriortotest;3) thetemperatureoftest,ifotherthanstandard1.aboratorytemperatureandthere1.ativehumidity；4) detai1.sofanyproceduresnotspecifiedinthisdocument;d) testresu1.ts:1) thenumberoftestpiecesused;2) theindividua1.andthemeantestresu1.ts；©ISO2024-A1.rightsreserved3) arecordoftheforce/distancecurve,quotingthepee1.strengthandthespreadofforcepeaksinaccordancewithISO6133;4) thec1.assification(1.ettersAtoE)andoptiona1.photographsofthefracturepatterns；5) forc1.assificationsA/D.B/DandCD.reportthepee1.ing1.ength;e) dateoftest.AnnexFePOrt.Aisanexamp1.eofthedocumentationoftheinjectionmou1.dingparametersandtheresu1.tsofthetestAnnexA(informative)Examp1.eof1.istingthetestresu1.tsA.1.Protoco1.forresu1.tsTab1.e,1.isasamp1.eprotoco1.fortheexpressionofresu1.ts.Tab1.eA.1.Examp1.eofprotoco1.Resu1.tsofpee1.testsinaccordancewith!SO813-2on.RigidsubstrateTPESoftcomponentswa1.1.thicknessDefectspresentonthetestspecimenStorageconditionsCurveshape(diagram)Pee1.strengthWstinNmm,withtheadhesionstrengthFandthesoftcomponentwidthbNumberoftestedspecimensSpreadofforcePeakS,inNC1.aSSifiCatiOn(AtoE)ofthefracturepatternwithco1.ourphotograph,ifnecessaryIndicationoftheinfectiondirectionofthesoftcomponentinproportiontotherigidsubstrateNon-standardconditionsA.2DescriptionOfinjectionmou1.dingparametersTab1.eA.2isanexamp1.eformforthedescriptionofprocessparameters.Tab1.e.2Descriptionofprocessparameters(injectionmou1.ding)ProcessparametersMateria1.ChosensettingThemateria1.smanufacturer'sspecificationAnnexB(normative)Ca1.ibrationschedu1.e8.1 InspectionBeforeanyca1.ibrationisundertaken,theconditionoftheitemstobeca1.ibratedsha1.1.beascertainedbyannspcctednmd)rcorded"aiHrnvived¾niihiQttonMantanticnftUtiau>fedtaiMbtadojXytvhethertheca1.ibrationItsha1.1.heascertainedthattheapparatusisgenera1.1.ytfortheintendedpurpose,inc1.udinganyparameters瞬fiedparametersaPProXi础&(M艇Ithena1.a符曲(三ic嘛慨e岫ew叫棚删眦bratedIfca1.ibrationprocedures.8.2 Schedu1.eVerification/CaHbraHonofthetestapparatusisamandatorypartofthisdocumentHowever,thefrequencybf1.f1.jtfihigMgHSOtittft>ta111.urCSaddncc.arc,un1.essotherwisestated,a1.thediscretionoftheindividua1.Theca1.ibrationschedu1.egiveninTab1.eB.1.hasbeencompi1.edby1.istinga1.1.theparametersspecifiedinthetest哪舱Utogett副mt森脚f联%用般甜酿韩gR三SFandn耨流岛踹惬翅Iate加mainForeachparameter,aca1.ibrationprocedureisindicatedbyreferencetoISO18899,toanotherpub1.icationca1.ibrationprocedurejVHtU1.JP1.514net1.ab1.V,hfrfftKnevftterence.morespecificordetai1.edTheverificationfrequencyforeachparameterisgivenbyacode-1.etter.Thecode-1.etterusedintheca1.ibrationschedu1.eis：S:standardinterva1.se1.ectedasgiveninISO18899.Tab1.eB.1.Ca1.ibrationfrequencyschedu1.eParameterRequirementSubc1.auseinISO18899:2013VerificationfrequencyguideNotespH1.tgtrnru1.cytoInadditiontotheitems1.istedinTab1.eB.1.,useofthefo1.1.owingisimp1.ied,a1.1.ofwhichneedca1.ibratinginaccordancewithISO18899:a) thermometerformonitoringtheconditioningandtesttemperatures;b) hygrometerformonitoringtheconditioningandtesthumidities;c) instrumentsfordeterminingdimensionsofthetestpiece.AnnexC(informative)G1.ossaryTab1.eC.1.TPEmateria1.specificdescriptionsTermDescriptionfracturepatternvisua1.eva1.uationofthetestpiecesurface(fracturepattern)fo1.1.owingthepee1.test.ThebbFsymbo1.Wadhesionstrength,inN.symbo1.Spee1.strength,inNmm.Bib1.iography1W(fQce2)rAtGeometrica1.productspecifications(GPS)Surfacetexture:Profi1.ePart1:Indicationof2 I5好W,K5W½¾B修陟6¾1.糊陀立Determina